HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 67918424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 57047250 | HCID 57047250 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67918424 | HCID 67918424 | — |
Reaction Steps
2.7 g of the compound of Example 20a and 1.3 g methyliodide were stirred in 30 ml dimethylformamide for 48 hours. Complete reaction by DC after that time. The dimethylformamide was distilled off and the residue stirred with ether yielding 3.3 g of the title compound, yellow solid. M.P.=192°-193° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112968 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-01b2bb7a695846e4901c7ccfe09d9beb |
| Source note | uspto-grants-1992_05 |