HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone → 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone | HCID 301557 | — |
| Reactant | Sodium hypobromite | HCID 23673712 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid | HCID 2759552 | 90% |
Reaction Steps
A solution of 18 g of 4-acetyl-4'-methoxybiphenyl in 285 ml of dioxane was oxidized with a dilute sodium hypobromite. Recrystallization from ethanol and acetic acid gave 4'-methoxybiphenyl-4-carboxylic acid melting at 285° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114613 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-815353fc731c4aa0a12ab6f1fe7a78a7 |
| Source note | uspto-grants-1992_05 |