HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → 4-(Octyloxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | Ethylparaben | HCID 8434 | — |
| Product | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
Reaction Steps
Using ethyl p-hydroxybenzoate (36.7 g, 0.22 mol) and n-octyl bromide (50 g, 0.26 mol), the reaction was carried out in the same manner as described in Example 13, (1), and then recrystallized from ethanol to give the title compound as a white micro-needles; yield: 43.0 g (71.6%); mp 100.2°-101.4° C. (the 1st mp), 107.0°-107.6° C. (the 2nd mp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114615 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-5268acb96c274bdfbf9a4b1e0ca086ff |
| Source note | uspto-grants-1992_05 |