Acetylacetone → HCID 53644755, compound

HRID 1196495Notes

Reaction equation

HRID 1196495 reaction equation
C(O)(=O)C(O)=O.[CH2:7]([O:11][C:12](=[O:27])[CH2:13][C:14]1[C:15]([NH2:26])=[N:16][NH:17][C:18]=1[C:19]1[CH:24]=[CH:23][C:22]([Cl:25])=[CH:21][CH:20]=1)[CH2:8]CC.[CH3:28][C:29](=O)[CH2:30][C:31](=O)[CH3:32]>Cl>[CH2:7]([O:11][C:12](=[O:27])[CH2:13][C:14]1[C:18]([C:19]2[CH:20]=[CH:21][C:22]([Cl:25])=[CH:23][CH:24]=2)=[N:17][N:16]2[C:31]([CH3:32])=[CH:30][C:29]([CH3:28])=[N:26][C:15]=12)[CH3:8]

Participants

4

Reactant 2

HCID 31261AcetylacetoneHCID 86745840HCID 86745840, compound

Product 1

HCID 53644755HCID 53644755, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

A solution of 35.5 g (0.089 mole) of 3-amino-5-(4-chlorophenyl)-1H-pyrazole-4-acetic acid butyl ester ethanedioate, 8.9 g (0.089 mole) of pentane-2,4-dione, and 10 ml of concentrated hydrochloric acid was stirred at room temperature for 17 hours under a nitrogen atmosphere.

Sources & evidence

ORD record
ord-96a195ad7c2b42d8950a30f0a2b777d8
Source dataset
uspto-grants-1992_05
Patent number
US05114944

Reaction notes

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