HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67896149, compound → HCID 19899009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67896149 | HCID 67896149 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19899009 | HCID 19899009 | 77.6% |
Reaction Steps
1 g of 3-(4-chlorophenyl)-4,5,6,7-tetrahydro-1,2-benzisoxazole-5,5-dicarboxylic acid was heated to 200°-210° C. for 5 minutes until effervescence had ceased. The residue was dissolved in ethanol and there was obtained from the solution 0.67 g of 3-(4-chlorophenyl)-4,5,6,7-tetrahydro-1,2-benzisoxazole-5-carboxylic acid of melting point 203°-205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05114960 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-76fc11d8131347aab3fe8237fc074d40 |
| Source note | uspto-grants-1992_05 |