HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → 2,3-Dibromopropionaldehydediethylacetal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | Propanoyl bromide, 2-bromo- | HCID 79047 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,3-Dibromopropionaldehydediethylacetal | HCID 4263567 | — |
Reaction Steps
7 g of 1,2-dibromo-propionaldehyde are added to a mixture of 5 g of ortho-formic acid triethyl-ester and 10 ml of ethanol. The solution is refluxed for 2 hours, remains standing for a night, then it is vacuum-distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116402 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-0d0a8735052f407fb6e773a75694f006 |
| Source note | uspto-grants-1992_05 |