HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 12504164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Chloral Hydrate | HCID 2707 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12504164 | HCID 12504164 | — |
Reaction Steps
Into an apparatus supplied with a Dean-Stark water separator 7 g of chloral hydrate, 10 g of butyl alcohol, 0.1 g of 4-methyl-benzene-sulphonic acid and 50 ml of benzene are weighed. The mixture is heated on a water-bath and the water separation is continued for 10 hours. The benzene is washed with water and sodium hydrogen carbonate, then distilled off and the product is vacuum distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116402 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-010456fb483541458293f0b94095fbe3 |
| Source note | uspto-grants-1992_05 |