HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromide ion → Ethane, 2-bromo-1,1-diethoxy-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromide ion | HCID 259 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Product | Ethane, 2-bromo-1,1-diethoxy- | HCID 74852 | — |
Reaction Steps
To a mixture of 10 g of vinyl acetate and 20 ml of carbon tetrachloride under cooling (temperature 10° C.) 10 ml of carbon tetrachloride and 18.5 g of bromide solution are added. 60 ml of ethanol are added to the mixture and it remains standing for 2 days. The organic phase is washed twice with 50 ml of water, then it is distilled in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116402 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-9ca5f762897d4da08106cabf3f5d88ce |
| Source note | uspto-grants-1992_05 |