p-Toluenesulfonic acid → HCID 19896177, compound

HRID 1196753Notes

Reaction equation

HRID 1196753 reaction equation
[CH2:1]([O:3][CH:4]([O:8][CH2:9][CH3:10])[CH:5]([Cl:7])[Cl:6])[CH3:2].C[C:12]1[CH:17]=[CH:16][C:15](S(O)(=O)=O)=[CH:14][CH:13]=1>C(O)CCCCCCC>[CH2:1]([O:3][CH:4]([O:8][CH2:9][CH2:10][CH2:12][CH2:17][CH2:16][CH2:15][CH2:14][CH3:13])[CH:5]([Cl:7])[Cl:6])[CH2:2][CH2:16][CH2:17][CH2:12][CH2:13][CH2:14][CH3:15]

Participants

4

Reactant 2

HCID 6101p-Toluenesulfonic acidHCID 120801,1-Dichloro-2,2-diethoxyethane

Product 1

HCID 19896177HCID 19896177, compound

Reagents, catalysts & solvents 1

HCID 9571-OctanolSolvent

Procedure

A mixture of 5 g of dichloro-acetaldehyde diethyl-acetal, 25 g of octanol and 0.1 g of 4-methyl-benzene-sulphonic acid is heated on a water-bath for 5 hours, then distilled.

Workup

  1. temperatureis heated on a water-bath for 5 hours
  2. distillationdistilled

Sources & evidence

ORD record
ord-a007cd5831c64be6a5e1ca3fabf5d5d7
Source dataset
uspto-grants-1992_05
Patent number
US05116402

Reaction notes

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