Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 19896626 | HCID 19896626 | — |
| Product | HCID 19896631 | HCID 19896631 | — |
Reaction Steps
A solution of 4-(methylthio)benzylazide (0.359 g, 2 mmol) in CH2Cl2 was cooled in ice and treated slowly with SO2Cl2 (0.297 g, 2.2 mmol). The reaction mixture was stirred at 5° C. for 1.5 h and then evaporated to dryness. The crude compound was obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05116833 |
|---|
| Source dataset | uspto-grants-1992_05 |
|---|
| ORD ID | ord-9fb9ef8bcf484da7b5714c0137e0e61e |
|---|
| Source note | uspto-grants-1992_05 |
|---|
