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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1196900Generated: October 31, 2026

HCID 19896765, compound → HCID 19896763, compound

https://huagongshe.com/reaction/1196900

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19896765HCID 19896765—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 19896763HCID 19896763—

Reaction Steps

2 g. 8,8-Dimethyl-2-(4-diethylamino-2-allyloxyphenyl)-5,6,7,8-tetrahydro-1H-imidazo[4,5-g]quinolin-6one were hydrogenated in ethanol in the presence of palladium/charcoal. After completion of the take up of hydrogen, the catalyst was filtered off, the filtration was evaporated and the residue recrystallized from isopropanol to give 1.8 g. of the title compound; m.p. 147°-148° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05116843
Source datasetuspto-grants-1992_05
ORD IDord-728abd536ba442f2b4062b2e40eac997
Source noteuspto-grants-1992_05