HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19896766, compound → HCID 19896776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19896766 | HCID 19896766 | — |
| Reactant | 4-Chloro-2-methoxybenzoyl chloride | HCID 22142450 | — |
| Product | HCID 19896776 | HCID 19896776 | 58% |
Reaction Steps
In a manner analogous to that described in EXAMPLE 2, from 4-chloro-2-methoxybenzoyl chloride and 4,4-dimethyl-6,7-diamino-1,2,3,4-tetrahydroquinolin-2-one (see Example 13 a)), after column chromatography, there was obtained a yield of 58% of theory of the title compound; m.p. 300°-303° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116843 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-0e4f8c8044364a3b9a11a628fa4ef650 |
| Source note | uspto-grants-1992_05 |