HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 57124953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 57311210 | HCID 57311210 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 57124953 | HCID 57124953 | 54% |
Reaction Steps
A mixture of 0.12 g of Isomer A of ethyl 4-[3-(4-oxo-2-thioxo-5-thiazolidinylidene)-1-butenyl]phenoxyacetate, 5 ml of water and 1 ml of 5% sodium hydroxide solution was stirred at room temperature for one hour. 10% hydrochloric acid was added to the mixture and the precipitated crystals were collected by filtration and washed with methanol to give Isomer A (54% yield) of 4-[3-(4-oxo-2-thioxo-5-thiazolidinylidene)-1-butenyl]phenoxyacetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116855 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-220c04e7455a4ca18c6ba01f36851d2b |
| Source note | uspto-grants-1992_05 |