化工社化工社 化学情報印刷レポート · 研究参考用
Formaldehyde → 4-(1-Methylethyl)-N-(2-thienylmethyl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | Thiophene | HCID 8030 | — |
| 反応物 | Benzamide, 4-(1-methylethyl)- | HCID 69277 | — |
| 溶媒 | Formic Acid | HCID 284 | — |
| 生成物 | 4-(1-Methylethyl)-N-(2-thienylmethyl)benzamide | HCID 4597909 | 80% |
反応手順
Thiophene (50 mmol), formaldehyde (10 mmol) and 4-isopropylbenzamide (10 mmol}were stirred in formic acid (10 ml) at 20° C. for four hours and treated in the same manner as in Example 2 to obtain N-(2-thienylmethyl)-4-isopropylbenzamide. Yield: 80%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05117000 |
| 出典データセット | uspto-grants-1992_05 |
| ORD ID | ord-81266c2dd6f944b9b8197a1d93de06ed |
| 出典メモ | uspto-grants-1992_05 |