HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycidol → HCID 22138552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | N-Methyloctadecylamine | HCID 75539 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22138552 | HCID 22138552 | 84% |
Reaction Steps
A mixture of glycidol (4 ml, 60 mmol) and N-methyl-octadecylamine (16 g, 60 mmol) in dry toluene (50 ml) was refluxed under stirring for 3 hours. After evaporation of the solvent, the residue was crystallized to yield 16 g (84%) of the title compound. m.p. 59° C. (Hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05116992 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-e0b597862f6d485f909f3d94728ab293 |
| Source note | uspto-grants-1992_05 |