HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1197189Generated: October 26, 2026
1,4-Dimethoxybenzene → Benzophenone, 2,2',5-trimethoxy-
https://huagongshe.com/reaction/1197189
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Dimethoxybenzene | HCID 9016 | — |
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Product | Benzophenone, 2,2',5-trimethoxy- | HCID 36279 | — |
Reaction Steps
A mixture of o-anisoyl chloride (25.8 g, 0.15 mmol) and 1,4-dimethoxybenzene (37.2 g, 0.27 mol) was heated for 20 hours at 200° C., under N2. Distillation led to recovered 1,4-dimethoxybenzene (18.7 g), b.p. 232° C. (8 mm) followed by the title product, shown below, (25.4 g, 63%), b.p. 232° C. (7 mm) which was suitable for carrying forward to the next step. ##STR3##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05117009 |
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| Source dataset | uspto-grants-1992_05 |
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| ORD ID | ord-60c5b63d54f94afa9db6efcd94c69946 |
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| Source note | uspto-grants-1992_05 |
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