HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19106825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 4-Chloro-1-nitro-2-(phenyl-2-propenyloxy)benzene | HCID 54410537 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Sodium Bicarbonate | HCID 516892 | — |
| Product | HCID 19106825 | HCID 19106825 | — |
Reaction Steps
The compound of Step A (7.2 g) was added to a suspension of tin (II) chloride (28 g) in ethanol (45 ml). The mixture was refluxed for 1.5 h. The reaction was diluted with ethyl acetate and neutralized by careful addition of saturated sodium bicarbonate solution. The organic solution was washed with brine and the solvent was dried over magnesium sulfate. Evaporation of the solution left a thick oil of the title compound (5.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05276039 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-96f2d859211a4ba4a05ce86de778481c |
| Source note | uspto-grants-1994_01 |