Formaldehyde → HCID 19107139, compound

HRID 1197516Notes

Reaction equation

[CH2:1]([OH:7])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[CH2:8]=[O:9].C1N2CN3[CH2:19][N:13](C2)CN1C3>>[CH2:1]([O:7][C:19]([O:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])([O:9][CH2:8][CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

Reactant 3

HCID 712Formaldehyde

HCID 4101Hexamethylenetetramine

HCID 81031-Hexanol

Product 1

HCID 19107139HCID 19107139, compound

Procedure

If the preferred raw materials are used in the process described above, in first step of the process n-hexanol was reacted with paraformaldehyde and hexamethylenetetramine to produce tris-hexoxymethanamine. In the second step of the process, phosphorus trichloride was reacted with neopentyl glycol in a mixture of neopentyl glycol and water to produce 5,5-dimethyl 1,3,2-dioxaphosphorinane-2-oxide. In the final step of the process the tris-hexoxymethanamine was reacted with the 5,5-dimethyl 1,3,2-dioxaphosphorinane-2-oxide to produce 5,5,5',5',5",5"-hexamethyl tris(1,3,2-dioxaphosphorinanemethan) amine 2,2',2"-trioxide.

Sources & evidence

ORD record: ord-e914a179523148d2bcebb06c9b6e27f7
Source dataset: uspto-grants-1994_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05276066

Reaction notes

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