HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19107030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Reactant | HCID 19107117 | HCID 19107117 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19107030 | HCID 19107030 | — |
Reaction Steps
A solution of the compound from Example 70 (1.0 g, 4.30 mmol) and diphenylphosphorylazide (1.3 g, 4.7 mmol) in 1.1 ml triethylamine and toluene was refluxed for 15 hours. Workup and silica gel chromatography gave the title compound (0.71 g) as a clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05276053 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-8a0a0c7f52174ef8bcbdf8f97b36776a |
| Source note | uspto-grants-1994_01 |