HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane → HCID 19106991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | 2-Bromobenzyl bromide | HCID 76965 | — |
| Reactant | 1-(3,6-Dihydro-2H-thiopyran-4-yl)pyrrolidine | HCID 13287468 | — |
| Product | HCID 19106991 | HCID 19106991 | 15% |
Reaction Steps
In a manner similar to that described in Example 82, 1-(3,6-dihydro-2H-thiopyran-4-yl)pyrrolidine (25.0 g, 0.15 mole) or as is in dioxane (100 ml) was treated with 2-bromobenzyl bromide (40.0 g, 0.16 mol) to give the title compound as a clear oil (16.3 g, 15%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05276053 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-8bbf473c2f2445c982a19874342cf0a9 |
| Source note | uspto-grants-1994_01 |