Lawesson's reagent → HCID 22098419, compound

HRID 1197567Notes

Reaction equation

HRID 1197567 reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH2:13][CH2:12][N:11]([C:14]3[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][C:22]([O:24][CH3:25])=[O:23])=[CH:16][CH:15]=3)[C:10]2=O)=[CH:5][CH:4]=1)#[N:2].COC1C=CC(P2(=S)SP(=S)(C3C=CC(OC)=CC=3)[S:36]2)=CC=1>C1(C)C(C)=CC=CC=1>[C:1]([C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH2:13][CH2:12][N:11]([C:14]3[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][C:22]([O:24][CH3:25])=[O:23])=[CH:16][CH:15]=3)[C:10]2=[S:36])=[CH:5][CH:4]=1)#[N:2]

Participants

4

Reactant 2

HCID 87949Lawesson's reagentHCID 15035944HCID 15035944, compound

Product 1

HCID 22098419HCID 22098419, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

Prepared by heating 1-(4-cyano-phenyl)-3-[4-(2-methoxycarbonyl-ethyl)-phenyl]-imidazolidin-2-one with 2,4-bis-(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetan-2,4-disulphide in xylene.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c651f71f49d743c79764a8c0420fd652
Source dataset
uspto-grants-1994_01
Patent number
US05276049

Reaction notes

Loading…