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HRID1197746

反应详情

EQUATION

反应方程式

HRID 1197746 的结构方程式

REACTANTS

反应物

2
结构：CCOP(OCC)OCC
HCID31215

Triethyl phosphite

C6H15O3P

结构：O=Cc1ccccc1CCl
HCID13826183

2-(Chloromethyl)benzaldehyde

C8H7ClO

PRODUCTS

生成物

1
结构：CCOP(=O)(Cc1ccccc1C=O)OCC
HCID19104780

未命名化合物

PROCEDURE

实验过程

47.9 g (0.31 mol) of 2-chloromethylbenzaldehyde were heated to 160° C. together with 51.5 g (0.31 mol) of triethyl phosphite. Ethyl chloride distilled off during the course of this. The product was purified by fractional distillation.

WORKUP

后处理

  1. distillationEthyl chloride distilled off during the course of this
  2. distillationThe product was purified by fractional distillation