HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → Diethyl 2-formylbenzylphosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 2-(Chloromethyl)benzaldehyde | HCID 13826183 | — |
| Product | Diethyl 2-formylbenzylphosphonate | HCID 19104780 | — |
Reaction Steps
47.9 g (0.31 mol) of 2-chloromethylbenzaldehyde were heated to 160° C. together with 51.5 g (0.31 mol) of triethyl phosphite. Ethyl chloride distilled off during the course of this. The product was purified by fractional distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278152 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-cc0f8c24a4c24503889bed2effd1d700 |
| Source note | uspto-grants-1994_01 |