HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Diethyl 2-formylbenzylphosphonate thiosemicarbazone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | Diethyl 2-formylbenzylphosphonate | HCID 19104780 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Diethyl 2-formylbenzylphosphonate thiosemicarbazone | HCID 53896642 | — |
Reaction Steps
2.0 g (8 mmol) of the compound A and 0.73 g of thiosemicarbazide were dissolved or suspended in 200 ml of absolute ethanol. 2 ml of acetic acid were added and the mixture was boiled under reflux for 3 h. In the course of the slow cooling, the product D precipitated in crystalline form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278152 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-3b6b3d1703714625b1121304484cd5ea |
| Source note | uspto-grants-1994_01 |