HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 19105159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 12,12,12-trifluorododecanoic Acid | HCID 9813738 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19105159 | HCID 19105159 | — |
Reaction Steps
Dissolve 12,12,12-trifluorododecanoic acid (244 mg, 0.96 mmol) in methylene chloride (5 mL) and add dimethylformamide (3 drops). Add oxalyl chloride (85 μL, 0.96 mmol) and stir until evolution of carbon dioxide is complete to give 12,12,12-trifluorododecanoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278171 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-248f6bbd21be480d8a0440942da7b465 |
| Source note | uspto-grants-1994_01 |