Thionyl Chloride → HCID 13432839, compound

HRID 1197870Notes

Reaction equation

HRID 1197870 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10](=O)[C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[CH:12]=2)=[CH:5][CH:4]=1.S(Cl)([Cl:23])=O>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N:9]=[C:10]([Cl:23])[C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[CH:12]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 306529N-(4-Methoxyphenyl)-3-nitrobenzaMide, 97%

Product 1

HCID 13432839HCID 13432839, compound

Procedure

Using the procedure of Step A of Example 1, 13 g of N-(4-methoxyphenyl)-3-nitrobenzamide prepared as in Step A of Example 1 and melting at 170° C. and 40 ml of thionyl chloride were reacted at reflux for 12 hours to obtain 14.5 g of N-(4-methoxyphenyl)-3-nitrobenzene-carboximidoyl chloride melting at 108° C.

Workup

  1. customwere reacted
  2. temperatureat reflux for 12 hours

Sources & evidence

ORD record
ord-33a80f6292bd4f4196d1a63f06e2b23d
Source dataset
uspto-grants-1994_01
Patent number
US05278180

Reaction notes

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