HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13432839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-(4-Methoxyphenyl)-3-nitrobenzaMide, 97% | HCID 306529 | — |
| Product | HCID 13432839 | HCID 13432839 | — |
Reaction Steps
Using the procedure of Step A of Example 1, 13 g of N-(4-methoxyphenyl)-3-nitrobenzamide prepared as in Step A of Example 1 and melting at 170° C. and 40 ml of thionyl chloride were reacted at reflux for 12 hours to obtain 14.5 g of N-(4-methoxyphenyl)-3-nitrobenzene-carboximidoyl chloride melting at 108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278180 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-33a80f6292bd4f4196d1a63f06e2b23d |
| Source note | uspto-grants-1994_01 |