Morpholine → HCID 67691201, compound

HRID 1197967Notes

Reaction equation

HRID 1197967 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH:12]1([C:18]([Cl:20])=O)[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1.Br[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]Cl.[NH:29]1[CH2:34][CH2:33][O:32][CH2:31][CH2:30]1>>[ClH:20].[CH:12]1([C:18]2[O:1][C:2]3[CH:7]=[CH:6][C:5]([O:8][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][N:29]4[CH2:34][CH2:33][O:32][CH2:31][CH2:30]4)=[CH:4][C:3]=3[C:9](=[O:11])[CH:10]=2)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]1

Participants

5

Reactant 4

HCID 8083MorpholineHCID 102792-AcetylhydroquinoneHCID 75938Cyclohexanecarbonyl chlorideHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 67691201HCID 67691201, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, cyclohexanecarbonyl chloride, 1-bromo-6-chlorohexane, and morpholine: mp 167°-168° C.

Sources & evidence

ORD record
ord-579dbe38f69c49bdbd989f399b01345e
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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