Dabco → HCID 14969213, compound

HRID 1198041Notes

Reaction equation

C(OC(=O)[CH2:5][C:6](=[O:25])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][O:18][CH:19]1[CH2:24][CH2:23][CH2:22][CH2:21][O:20]1)C.N12CCN(CC1)CC2>>[O:20]1[CH2:21][CH2:22][CH2:23][CH2:24][CH:19]1[O:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][C:6](=[O:25])[CH3:5]

Participants

Reactant 2

HCID 9237Dabco

HCID 14969216HCID 14969216, compound

Product 1

HCID 14969213HCID 14969213, compound

Procedure

The title compound was prepared from 3-oxo-14-[(tetrahydro-2H-pyran-2-yl)oxy]-tetradecanoic acid ethyl ester (7.97 g, 0.021 mol), 1,4-diazabicyclo-[2.2.2]octane (24.13 g, 0.215 mol), and xylenes (39.3 mL, 15 eq) using the procedure described in Example 3, Step B.

Sources & evidence

ORD record: ord-a16cdc0bf8434edf89c6b4a2b6fc39b4
Source dataset: uspto-grants-1994_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05278326

Reaction notes

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