HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pentadecanone → N-[2,6-bis(1-methylethyl)phenyl]-3-oxo-hexadecanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pentadecanone | HCID 61303 | — |
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Product | N-[2,6-bis(1-methylethyl)phenyl]-3-oxo-hexadecanamide | HCID 9980090 | — |
Reaction Steps
The title compound was prepared from 2-pentadecanone (3.0 g, 0.013 mol), 2,6-diisopropylphenyl isocyanate (2.64 g, 0.013 mol), and lithium diisopropylamide (0.013 mol) using the procedure described in Example 1. Purification by flash chromatography (silica gel, 15% EtOAc/hexane) yielded 1.92 g (0.004, 34%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-7c236d1f04934887a673b1afa88c474b |
| Source note | uspto-grants-1994_01 |