HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Undecanone → HCID 10317246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Undecanone | HCID 8163 | — |
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Product | HCID 10317246 | HCID 10317246 | — |
Reaction Steps
The title compound was prepared from 2-undecanone (5.0 g, 0.029 mol), 2,6-diisopropylphenyl isocyanate (5.96 g, 0.029 mol), and lithium diisopropylamide (0.029 mol) using the procedure described in Example 1. The desired product was obtained in 79.4% yield (8.6 g, 0.023 mol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-ed253bd5f3074f5aa0a569a2b6e40ec6 |
| Source note | uspto-grants-1994_01 |