HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexadecan-2-one → HCID 10366149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexadecan-2-one | HCID 29251 | — |
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Product | HCID 10366149 | HCID 10366149 | — |
Reaction Steps
The title compound was prepared from 2-hexadecanone (5.0 g, 0.018 ml), 2,6-diisopropylphenyl isocyanate (3.72 g, 0.018 mol), and lithium diisopropylamide (0.018 mol) using the procedure described in Example 1. The desired product was obtained in 80% yield (6.38 g, 0.014 mol). MS: 443 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-88407132d23747e6b7dd8cb5b7ebc263 |
| Source note | uspto-grants-1994_01 |