HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 54556855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3,4-dihydro-2H-pyran | HCID 8080 | — |
| Reactant | ethyl 5-hydroxy-3-oxo-5,5-diphenylpentanoate | HCID 255514 | — |
| Product | HCID 54556855 | HCID 54556855 | — |
Reaction Steps
The title compound (J. W. Wolfe, et al, J. Org. Chem. 29, 3249 (1964) ) was prepared from δ-hydroxy-β-oxo-δ-phenylbenzenepentanoic acid ethyl ester (2.0 g, 0.006 mol), p-toluenesulfonic acid (0.014 g, 0.60 mmol), and 3,4-dihydro-2H-pyran (0.77 g, 0.009 mol) using the procedure described in Example 6, Step A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-d576f722625042c7a04eefde12a66917 |
| Source note | uspto-grants-1994_01 |