HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pentadecanone → 3-oxo-N-(2,4,6-trimethoxyphenyl)pentadecanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pentadecanone | HCID 61303 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | 2,4,6-Trimethoxyphenyl isocyanate | HCID 10081812 | — |
| Product | 3-oxo-N-(2,4,6-trimethoxyphenyl)pentadecanamide | HCID 19105579 | — |
Reaction Steps
The title compound was prepared from 2-pentadecanone (0.54 g, 0.0023 mol), 2,4,6-trimethoxyphenyl isocyanate (prepared from 2,4,6-trimethoxyaniline hydrochloride and phosgene (2.5 eq)) and lithium diisopropylamide (0.0023 mol) using the procedure described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05278326 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-e13e89574a66432f8b4cff609a0ab57c |
| Source note | uspto-grants-1994_01 |