HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Diethylamino)sulfur trifluoride → HCID 19103976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Diethylamino)sulfur trifluoride | HCID 123472 | — |
| Reactant | HCID 19103983 | HCID 19103983 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19103976 | HCID 19103976 | — |
Reaction Steps
In 30 ml of dichloromethane was dissolved 1.0 g of 5-chloro-6-(1-hydroxyethyl)-4-[1-(4-difluoromethoxyphenyl)-ethylamino]pyrimidine, and to the mixture was added dropwise 0.4 g of diethylaminosulfur trifluoride under ice cooling. The mixture was stirred at room temperature for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05280025 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-cf42cba7616246ed8eacaab91057ac9b |
| Source note | uspto-grants-1994_01 |