Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → HCID 67820861, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | Ethyl Acetate | HCID 8857 | — |
| 반응물 | Ethyl Acetoacetate | HCID 8868 | — |
| 반응물 | Benzaldehyde, 4-octyl- | HCID 2734685 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 67820861 | HCID 67820861 | — |
반응 단계
Ethyl acetoacetate (11.8g, 0.092 moles), paraoctylbenzaldehyde (10.0 g, 0.046 moles) and piperidine (1.5ml) were stirred for 48 hrs. at room temperature. Ethyl acetate (50ml) was added and the solution was added to water (100ml). The layers were separated and the organic layer dried over anhydrous sodium sulfate, filtered and concentrated to an oily solid. The title products were separated and purified by silica gel chromatography. The structure assignments were supported by NMR, infrared spectra and elemental analysis (330.5)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05280047 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-4de7432c9af44b5c9f07a058e807f325 |
| 출처 메모 | uspto-grants-1994_01 |