HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl-beta-alanine tert-butyl ester → N-Acetyl-beta-alanine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl-beta-alanine tert-butyl ester | HCID 19102537 | — |
| Reactant | Ethanol ammonium hydroxide water | HCID 86596525 | — |
| Product | N-Acetyl-beta-alanine | HCID 76406 | 116.4% |
Reaction Steps
Utilizing the procedure for converting 40a to 41a, 127 (0.10 g, 0.19 mmol) gave 128 (29 mg, 39%) as a fluffy solid after flash chromotography (silica, 10:1.2:1.2 ethanol/H2O/NH4OH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281585 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-5c03653d43c04599bcc91a5a20e574d6 |
| Source note | uspto-grants-1994_01 |