HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 19102590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 19102579 | HCID 19102579 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19102590 | HCID 19102590 | — |
Reaction Steps
Solid sodium borohydride (0.11 g, 2.89 mmol) was added to a stirred suspension of 1-[α-phenyl-3-{2(E)-(quinolin-2-yl)ethenyl}benzyl]indole-6-carboxaldehyde (0.32 g, 0.69 mmol) in methanol (10 ml) and the mixture was stirred for 30 minutes giving a clear solution which was poured onto ammonium chloride solution and extracted with dichloromethane. The extract was dried and evaporated to give a solid product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281593 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-d8580186d5a745769d4cbb9236998ebd |
| Source note | uspto-grants-1994_01 |