HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 1551028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Cyclopentanone | HCID 8452 | — |
| Product | HCID 1551028 | HCID 1551028 | — |
Reaction Steps
The procedure was similar to that in Example 4 by reacting benzaldehyde with the morpholine enamine of cyclopentanone to give 2-(E)-benzylidene cyclopentanone. The melting point of this intermediate compound was determined to be 67°-69° C. A subsequent Mannich reaction yielded the 2-Dimethylaminomethyl-5-(E)-benzylidene cyclopentanone hydrochloride. The melting point of the product was determined to be 153°-155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281622 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-7b17cdb3643e4b8fb4fc178aafedf10e |
| Source note | uspto-grants-1994_01 |