HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanone → HCID 10726798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanone | HCID 8452 | — |
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Product | HCID 10726798 | HCID 10726798 | — |
Reaction Steps
The procedure was similar to that in Example 4 by reacting 2-methoxybenzaldehyde with the morpholine enamine of cyclopentanone to give 2-(E)-[(2-methoxy) benzylidene] cyclopentanone. The melting popint of this intermediate compound was determined to be 80°-82° C. A subsequent Mannich reaction yielded the 2-Dimethylaminomethyl-5-(E)-[(2-methoxy) benzylidene] cyclopentanone hydrochloride. The melting point of the product was determined to be 167°-169° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281622 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-483d53159fdf4fbaba7042b9169fc375 |
| Source note | uspto-grants-1994_01 |