HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 135703694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | HCID 10081379 | HCID 10081379 | — |
| Product | HCID 135703694 | HCID 135703694 | — |
Reaction Steps
Condensation of 2-(1,3-dioxolanyl)-4-methyl-5-hydroxyaminopyridine with thiosemicarbazide in the presence of concentrated hydrochloric acid, followed by treatment with sodium bicarbonate afforded the desired 5-hydroxyamino-4-methyl-2-formylpyridine thiosemicarbazone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281715 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-0f8aff5afa5a4b5e8b14bacb08c1bd21 |
| Source note | uspto-grants-1994_01 |