HCID 123850930, compound → HCID 19103285, compound

Participants

Reaction Conditions

Reaction Steps

Comparison Example 2. Into a glass tube with an outside diameter of 10 mm and a length of 10 cm were introduced 0.002 mL of a 20 weight % isopropanolic chloroplatinic acid solution and 2 mL of a mixture of 1 part N-dimethylsilyldiallylamine and 3 parts benzene, and the tube was sealed. The tube was heated for 17 hours at 80° C. The conversion of starting material was 100 weight %. 1-Allyl-2,2,3-trimethyl-1-aza-2-silacyclobutane and 1-allyl-2,2-dimethyl-1-aza -2-silacyclopentane were produced in a molar ratio of 66:34 and a combined yield of 55%.

Provenance & Evidence