Hydrogen Peroxide → HCID 15634753, compound

Participants

Reaction Steps

A solution of 8.4 g (0.04 mole) of 3-methyl-2-aminobenzophenone, 150 ml of acetic acid and 40 ml of 30% hydrogen peroxide was allowed to stand at ambient temperature for 3 days and the resulting solution was poured into 800 ml of ice-water mixture. The solid which precipitated was collected by filtration, washed with water and dried. This solid was recrystallized twice from isopropanol to yield 4.1 g (49%) of tan crystals, m.p. 73°-75° C.

Provenance & Evidence