HCID 15634761, compound → HCID 14835357, compound

HRID 1198992Notes

Reaction equation

HRID 1198992 reaction equation
[CH2:1]([C:3]1[C:4]([NH2:17])=[C:5]([CH:14]=[CH:15][CH:16]=1)[C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:7])[CH3:2]>C(O)(=O)C.OO>[CH2:1]([C:3]1[C:4]2[C:5](=[C:6]([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)[O:7][N:17]=2)[CH:14]=[CH:15][CH:16]=1)[CH3:2]

Participants

4

Reactant 1

HCID 15634761HCID 15634761, compound

Product 1

HCID 14835357HCID 14835357, compound

Reagents, catalysts & solvents 2

HCID 176Acetic AcidSolventHCID 784Hydrogen PeroxideSolvent

Procedure

A solution of 7.5 g (0.033 mole) of 3-ethyl-2-aminobenzophenone in 150 ml of acetic acid and 40 ml of 30% hydrogen peroxide was let stand at ambient temperature for 72 hr. The solution was poured into ice water and a solid gradually crystallized. The solid was collected by filtration, washed with water and dried. The solid was then slurried with 20 ml of carbon tetrachloride and the mixture was filtered.

Workup

  1. customa solid gradually crystallized
  2. filtrationThe solid was collected by filtration
  3. washwashed with water
  4. customdried
  5. filtrationthe mixture was filtered

Sources & evidence

ORD record
ord-c0141e6713d94e4f99b92099a6bad3a7
Source dataset
uspto-grants-1990_02
Patent number
US04898874

Reaction notes

Loading…