Hydrogen Peroxide → HCID 14835365, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 130 ml of 30% hydrogen peroxide in 350 ml of glacial acetic acid was heated on a steam bath for 1 hr. To the cooled solution was added a solution of 31.0 g (0.11 mole) of (2-amino-3-methylphenyl)(4-bromophenyl)methanone in 400 ml of glacial acetic acid. The reaction mixture was heated to 95° C. to dissolve all solids, then heated at 65°-70° C. for 4 hr and let stand at ambient temperature overnight.

Provenance & Evidence