Hydrogen Peroxide → HCID 14835385, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 150 ml of 30% hydrogen peroxide and 300 ml of glacial acetic acid was heated on a steam bath for 1 hr and then cooled. The solution was treated with 26.3 g (0.094 mole) of (2-amino-3-methylphenyl) [4-(trifluoromethyl)phenyl]methanone and the mixture was heated at 70° C. for 7 hr and let stand at ambient temperature overnight. The mixture was poured into 2 liters of ice water and the solid was collected by filtration, washed with water and recrystallized from 2-propanol to yield 3.4 g (13%) of tan powder, m.p. 118°-119° C.

Provenance & Evidence