Methylamine → HCID 19867813, compound

Participants

Reaction Steps

The title compound is prepared by reacting the acid chloride of 5-chloro-3-phenyl-2,1-benzisoxazole-7-acetic acid and excess monomethylamine in a closed container in an aprotic solvent. The unused methylamine is allowed to escape and the solution is washed with hydrochloric acid followed by aqueous base and evaporated. The title compound is obtained by conventional crystallization from alkanolic solution or by chromatography.

Provenance & Evidence