HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Methoxyphenyl)but-3-en-2-one → 4-(3-Methoxyphenyl)butan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Methoxyphenyl)but-3-en-2-one | HCID 182007 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(3-Methoxyphenyl)butan-2-one | HCID 11423902 | 99.2% |
Reaction Steps
A solution of 30.1 g of 4-(3-methoxyphenyl)-3-buten-2-one in 200 ml of MeOH was hydrogenated over 200 mg of 10% palladium on carbon for two hours. The catalyst was filtered and the solvent evaporated in vacuo to give 30.2 g of yellow oily 4-(3-methoxyphenyl)-2-butanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04898889 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-61ca01d144964a2e98ce71468bfe29b1 |
| Source note | uspto-grants-1990_02 |