HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 16beta-Methyl-5-androsten-17beta-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 16beta-Methly-5-androsten-17-one | HCID 54347812 | — |
| Product | 16beta-Methyl-5-androsten-17beta-ol | HCID 70359444 | — |
Reaction Steps
Sodium borohydride is added to the 16β-methly-5-androsten-17-one(produced in F hereinabove) according to the procedure described in Example 8F to form mostly the above-identified final product and a smaller amount of 16β-methly-5-androsten-17α-ol which are separated by HPLC on a silica gel column.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04898694 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-6ad008fadd014ccbb68ae5c1b8ee0691 |
| Source note | uspto-grants-1990_02 |