反应详情

温度

57 °C

To a 250-ml round bottom flask fitted with a condenser, heater, stirrer and feed control, is charged a mixture of 60.0 g of acetone and 0.1 g of Engelhard Clay-24. The mixture is heated to reflux (57° C.) with stirring, and 40.0 g of "80%" cumene hydroperoxide solution added dropwise such that the pot temperature does not exceed 66° C.

1. customTo a 250-ml round bottom flask fitted with a condenser
2. additionheater, stirrer and feed control, is charged
3. temperatureThe mixture is heated
4. customdoes not exceed 66° C.